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. 2023 Jun 30;15(13):2898.
doi: 10.3390/polym15132898.

Optimal Design of Multi-Scale Fibre-Reinforced Cement-Matrix Composites Based on an Orthogonal Experimental Design

Affiliations

Optimal Design of Multi-Scale Fibre-Reinforced Cement-Matrix Composites Based on an Orthogonal Experimental Design

Kaixin Qiu et al. Polymers (Basel). .

Abstract

Cement-matrix composite are typical multi-scale composite materials, the failure process has the characteristics of gradual, multi-scale and multi-stage damage. In order to delay the multi-stage damage process of cement-matrix composites, the defects of different scales are suppressed by using different scales of fibres and fly ash (FA), and the overall performance of cement-matrix composites is improved, a new multi-scale fibre-reinforced cement-based composite composed of millimetre-scale polyvinyl alcohol fibre (PVA), micron-scale calcium carbonate whisker (CW), and nano-scale carbon nanotubes (CNTs) was designed in this study. The compressive strength, flexural strength, splitting tensile strength, and chloride ion permeability coefficient were used as assessment indices by the orthogonal test design. The impacts of the three fibre scales and fly ash on each individual index were examined, and the overall performance of the multi-scale fibre-reinforced cementitious materials (MSFRCC) was then optimized using grey correlation analysis. The optimized mix ratio for overall performance was PVA: 1.5%, CW: 2%, CNTs: 0.1%, FA: 40%. Compared with the optimal results for each group, the compressive strength of the final optimized MSFRCC group decreased by 8.9%, the flexural strength increased by 28.4%, the splitting tensile strength increased by 10%, and the chloride ion permeability coefficient decreased by 5.7%. The results show that the compressive performance and resistance to chloride ion penetration of the optimized group are slightly worse than those of the optimal group in the orthogonal test, but its flexural performance and splitting tensile performance are significantly improved.

Keywords: MSFRCC; fly ash; grey correlation analysis; multi-scale fibres; orthogonal experiments.

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Conflict of interest statement

The authors declare no conflict of interest.

Figures

Figure 1
Figure 1
Dispersion-treated CNTs solution and undispersion-treated CNTs solution.
Figure 2
Figure 2
Experimental design flow chart.
Figure 3
Figure 3
Effect of various factors on the compressive strength.
Figure 4
Figure 4
Contribution rate of each influencing factor to compressive strength.
Figure 5
Figure 5
Effect of various factors on the flexural strength.
Figure 6
Figure 6
Contribution rate of each influencing factor to flexural strength.
Figure 7
Figure 7
Effect of various factors on the splitting tensile strength.
Figure 8
Figure 8
Contribution rate of each influencing factor to splitting tensile strength.
Figure 9
Figure 9
Effect of various factors on the chloride ion permeability coefficient.
Figure 10
Figure 10
Contribution rate of each influencing factor to chloride ion permeability coefficient.
Figure 11
Figure 11
Effect of various factors on the grey correlation degree.

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