Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2025 Apr 24;10(Pt 4):x250364.
doi: 10.1107/S2414314625003645. eCollection 2025 Apr.

2-[(5-Methyl-1,3,4-thia-diazol-2-yl)sulfan-yl]- N'-(4-nitro-benzyl-idene)acetohydrazide monohydrate

Affiliations

2-[(5-Methyl-1,3,4-thia-diazol-2-yl)sulfan-yl]- N'-(4-nitro-benzyl-idene)acetohydrazide monohydrate

Murugan Nidhishree et al. IUCrdata. .

Abstract

In the title hydrate, C12H11N5O3S2·H2O, the dihedral angle between the aromatic rings is 9.6 (3)°. In the crystal, N-H⋯O and O-H⋯N hydrogen bonds link the components into (101) sheets.

Keywords: 1,3,4-thia­diazole; crystal structure; hydrogen bonds.

PubMed Disclaimer

Figures

Figure 1
Figure 1
The mol­ecular structure of (I) with displacement ellipsoids drawn at the 50% probability level.
Figure 2
Figure 2
Part of a supra­molecular layer in the crystal of (I) showing various supra­molecular motifs. Symmetry codes (i) −1 + x, y, z; (ii) −x, −y, −z; (iii) formula image + x, formula image − y, −formula image + z; (iv) −formula image + x, formula image − y, −formula image + z; (v) 1 − x, −y, 1 − z].

References

    1. Altıntop, M. D., Can, Ö. D., Demir Özkay, Ü. & Kaplancıklı, Z. A. (2016). Molecules, 21, 1004.
    1. Anthwal, T. & Nain, S. (2022). Front. Chem.9, 671212–671212. - PMC - PubMed
    1. Bhinge, S. D., Chature, V. & Sonawane, L. V. (2015). Pharm. Chem. J.49, 367–372.
    1. Bruker (2016). APEX2 and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Cason, C. J. (2004). POV-RAY. Persistence of Vision Raytracer Pty. Ltd, Victoria, Australia.

LinkOut - more resources